Image analysis as an improved melting criterion in laser-heated diamond anvil cell (1506.06786v1)

Abstract: The precision of melting curve measurements using laser-heated diamond anvil cell (LHDAC) is largely limited by the correct and reliable determination of the onset of melting. We present a novel image analysis of speckle interference patterns in the LHDAC as a way to define quantitative measures which enable an objective determination of the melting transition. Combined with our low-temperature customized IR pyrometer, designed for measurements down to 500K, our setup allows studying the melting curve of materials with low melting temperatures, with relatively high precision. As an application, the melting curve of Te was measured up to~$\rm35\,GPa$. The results are found to be in good agreement with previous data obtained at pressures up to~$\rm10\,GPa$.